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Beilstein J. Org. Chem. 2014, 10, 2724–2728, doi:10.3762/bjoc.10.287
Graphical Abstract
Figure 1: Structure of the pentasaccharide repeating unit of the O-specific polysaccharide of E. coli O117:K9...
Figure 2: Structure of the synthesized pentasaccharide (1) and its precursor intermediates.
Scheme 1: Reagents and conditions: (a) (i) acetic anhydride, pyridine, room temperature, 2 h; (ii) NaBH3CN, H...
Scheme 2: Reagents: (a) N-iodosuccinimide (NIS), TMSOTf, CH2Cl2, MS 4 Å, −30 °C, 1 h, 72%; (b) HClO4/SiO2, CH3...
Beilstein J. Org. Chem. 2014, 10, 293–299, doi:10.3762/bjoc.10.26
Figure 1: Structure of the synthesized tetrasaccharide and its precursor intermediates. PMB: p-methoxybenzyl.
Scheme 1: Reagents and conditions: (a) 2,2-dimethoxypropane, p-TsOH, DMF, room temperature, 12 h; (b) acetic ...
Scheme 2: Reagents: (a) N-iodosuccinimide (NIS), TfOH, CH2Cl2, MS 4 Å, −30 °C, 1 h, then 0 °C, 1 h, 77%; (b) ...